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antibacterial .ai

Method reference

High throughput screening for antibacterials, and why the library should be cut first

Whole-cell antibacterial screens have a famously low hit rate. The economics improve enormously when the library is triaged before it reaches a plate.

At a glance

Formats
96, 384 and 1536 well plates
Read-out
Growth inhibition, whole cell
Known problem
Very low hit rates for Gram-negatives
Cheapest fix
Cut the library before the plate

High throughput screening is the practice of testing large compound libraries against a biological read-out in miniaturised, automated format. In antibacterial discovery it works, but the economics are unusually brutal, and the reason is worth understanding before designing a campaign.

The mechanics

  • Plate formats. 96 well for careful work, 384 for most campaigns, 1536 where volumes and cost force it.
  • Read-out. For antibacterials the primary read is growth inhibition, measured by optical density or by a metabolic indicator such as resazurin. Whole cell, phenotypic, no target required.
  • Controls. Every plate carries growth and sterility controls plus a reference agent, because plate to plate variation is the main source of false calls.
  • Confirmation. Primary hits go to a dose response, then to a proper MIC determination. A primary hit is a hypothesis, not a result.

Why antibacterial screens have such low hit rates

Target based screening dominated the 1990s and early 2000s and produced very few clinical antibacterials. The reason is now well documented: compounds that inhibit a purified essential enzyme frequently fail to reach that enzyme inside a living cell. The bacterial envelope, and especially the Gram-negative outer membrane, filters out most of medicinal chemistry's usual chemical space.

Whole cell screening avoids that failure mode by testing the real question directly, but it pays for it in two ways: the hit rate against Gram-negatives is very low, and a hit arrives with no mechanism attached. You then have to work out what it hits, which is its own project.

The chemical space problem

Compounds that accumulate in Gram-negative bacteria tend to be small, polar and to carry an ionisable amine, which is close to the opposite of a typical drug-like screening library optimised for oral absorption in humans. A conventional corporate library is therefore not a good antibacterial library, and screening more of it does not fix that. The Gram-negative bacteria page covers the accumulation rules in detail.

What a campaign actually costs

Costs vary enormously with format, compound supply and whether the work is internal or contracted, so treat the shape rather than the number as the point:

StageWhat drives the costWhat triage changes
Primary screenPlates, reagents, compound supply, instrument timeFewer plates for the same decision
Hit confirmationDose response in triplicateFewer false leads reaching this stage
MIC panelOne plate per organism per compoundPanel scoped to organisms with a real chance
Mechanism workResistant mutant generation, sequencing, imagingStarts with a hypothesis instead of nothing
Calendar timeQueueing, repeats, reagent lead timesWeeks removed at the front

Triage before the plate

In silico triage does not replace a screen. It changes what goes into it. Three things are worth deciding before a library reaches a plate:

  1. Is the scaffold already known to fail? If the closest published analogs have no Gram-negative activity, the series will need a permeability strategy, not more plates.
  2. Which organisms belong in the panel? Running six organisms when the compound class has a realistic chance against two is a way to spend five sixths of the budget confirming what was predictable.
  3. Which analogs actually differ? A series often contains many compounds that will behave identically. Ranking removes the duplicates before they consume wells.

The output of that triage is a shorter plate list with a written reason for each inclusion. That is also what makes the result defensible in a program review, which matters as much as the wells saved.

Where imaging read-outs fit

A growth curve says whether a compound worked. Imaging based high content screening can say something about how, by reading the shape and organisation of the treated cells. It costs more per well and it answers the mechanism question earlier, which is the trade a program makes deliberately rather than by default.

Screen a compound now

The screen below runs the triage step on one compound against a six strain panel. It returns a predicted band per strain with the resistance mechanism named, which is the input to deciding what the real campaign should contain. Details of the method are on the how it works page.

Run it

Screen a compound against a six-strain panel

The panel below is preselected for this page. Change the compound, run it, and read the matrix. Three screens per session, no account needed.

Run a screen

of 3 left

Strain panel

No account needed. 3 screens per session.

Ready to run CC1(O)C2CC3C(N(C)C)C(O)=C(C(N)=O)C(=O)C3(O)C(O)=C2C(=O)c2c(O)cccc21 ESKAPE panel
Nothing predicted until you run
Strain MIC (µg/mL) Call Resistance risk Conf.
Tick at least one strain in the panel on the left.

Nothing here is predicted yet

These are the strains this page preselected, waiting on a compound. Run the screen and every row fills in with an MIC band, an S / I / R call, the mechanism expected to decide it and a confidence out of four.

Strain MIC (µg/mL) Call Resistance risk Conf.

Why

Closest published analogs

Save this screen and run the rest of your series. screen left in this session. This session is used up.

Computational prediction from published literature. Research use only, not a lab measurement and not clinical guidance.

Take it from reading to a read-out

Run a screen on the compound this page made you think about, then create an account when you want to keep the result and bring the series.

Run a screen first

What you are agreeing to

  • Your compounds stay yours
  • Never used for model training
  • Deletable on request
  • No card required to run a screen

Screen your own compound.
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